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91.
FENGZhi-min LIFeng CHENRong ZHUXiao-juan LIXiao-ru 《高等学校化学研究》2004,20(3):270-273
The present paper covers the synthesis and the characterization of ligand 2-decyl-3, 6, 9-tris (car-boxymethyl)-3,6,9-triazaundecan-1,11-dioic acid, HsL, and its Gd (Ⅲ) chelate. The protonation constantsfor HsL(IgKi^H= 10. 90, 8.50, 4.55, 2.92., 2.20) and the stability constant for GdL^2- (lgKGdL^2- = 2.2.80)were determined by means of potentiometric titration. They are similar to the corresponding values of DTPAand Gd-DTPA, respectively. The results obtained show that the basicity of the ligand and the stability con-stant of its Gd (Ⅲ) chelate are not obviously altered after the introduction of a linear chain decyl group intothe terminal acetic acid residue of DTPA. The Gd(Ⅲ) chelate may be a potential contrast agent with liver-specificity for magnetic resonance imaging(MRI). 相似文献
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A newly developed multi-axial testing technique for sheet materials is employed to investigate the inelastic response of a temper-rolled stainless steel 301LN under isothermal quasi-static loading conditions at room temperature. The experimental technique consists of a flat sheet specimen, which is subject to combinations of shear and normal loading using a custom-made dual-actuator system. The large deformation behavior under monotonic loading is determined along more than 20 distinct radial paths in the stress space. The experimental results indicate that Hill's quadratic yield function along with an associated flow rule provides a good approximation of the initial yield behavior of this anisotropic two-phase FCC/BCC sheet material. Based on the experimental data for radial monotonic loading, it is concluded that conventional isotropic-kinematic hardening models cannot successfully describe the strain hardening of this austenitic steel. Instead, a non-associated anisotropic hardening model is proposed that relates the increase in yield strength to an isothermal martensitic transformation kinetics law. The comparison of the model predictions with the experimental results shows very good agreement for all biaxial and uniaxial experiments. 相似文献
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From the linear Vlasov equation,the theoretical investigation on relativistic backward wave osciUator is performed.The relationship between the microwave power and the guiding magnetic field,which accords with the results of the particle simulation and experiments,is deduced. 相似文献
96.
Pump−probe experiments at the TEMPO beamline using the low‐α operation mode of Synchrotron SOLEIL 下载免费PDF全文
Mathieu G. Silly Tom Ferté Marie Agnes Tordeux Debora Pierucci Nathan Beaulieu Christian Chauvet Federico Pressacco Fausto Sirotti Horia Popescu Victor Lopez-Flores Marina Tortarolo Maurizio Sacchi Nicolas Jaouen Philippe Hollander Jean Paul Ricaud Nicolas Bergeard Christine Boeglin Bharati Tudu Renaud Delaunay Jan Luning Gregory Malinowski Michel Hehn Cédric Baumier Franck Fortuna Damjan Krizmancic Luigi Stebel Rudi Sergo Giuseppe Cautero 《Journal of synchrotron radiation》2017,24(4):886-897
The SOLEIL synchrotron radiation source is regularly operated in special filling modes dedicated to pump–probe experiments. Among others, the low‐α mode operation is characterized by shorter pulse duration and represents the natural bridge between 50 ps synchrotron pulses and femtosecond experiments. Here, the capabilities in low‐α mode of the experimental set‐ups developed at the TEMPO beamline to perform pump–probe experiments with soft X‐rays based on photoelectron or photon detection are presented. A 282 kHz repetition‐rate femtosecond laser is synchronized with the synchrotron radiation time structure to induce fast electronic and/or magnetic excitations. Detection is performed using a two‐dimensional space resolution plus time resolution detector based on microchannel plates equipped with a delay line. Results of time‐resolved photoelectron spectroscopy, circular dichroism and magnetic scattering experiments are reported, and their respective advantages and limitations in the framework of high‐time‐resolution pump–probe experiments compared and discussed. 相似文献
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马长兴 《数学物理学报(A辑)》2000,20(1):25-30
(7)中给出并研究了均匀设计抽样(UDS)及随机化均匀设计(RUD)的一些优良性质,作者给出该设计和抽样的一、二阶矩。 相似文献
100.
在物理实验中引入“计算机应用”是当前教改的任务之一。也是实验教学发展的必然趋势。本通过重力加速度和型材杨氏模量的测量实验,说明计算机通信接口在物理实验中应用的可行性。 相似文献